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Hyodeoxycholic acid

Hyodeoxycholic acid Basic information
Product Name:Hyodeoxycholic acid
Synonyms:7-deoxyhyocholicacid;alpha-hyodeoxycholicacid;3α,6α-Dihydroxy-5β-cholanoic acid;Hyodeoxycholic;3à,6à-dihydroxy-5á-cholan-24-oic acid;3a,6a-Dihydroxy-5b-Cholan-24-Oic Acid;HYODEOXYCHOLIC ACID FREE ACID;HYODEOXYCHOLIC ACID 98%
CAS:83-49-8
MF:C24H40O4
MW:392.58
EINECS:201-483-2
Product Categories:Inhibitors;reference standards from Chinese medicinal herbs (TCM).;Intermediates & Fine Chemicals;Isotope Labelled Compounds;Herb extract;standardized herbal extract;Natural Plant Extract;Metabolites & Impurities;Pharmaceuticals;Steroids;chemical reagent;pharmaceutical intermediate;phytochemical
Mol File:83-49-8.mol
Hyodeoxycholic acid Structure
Hyodeoxycholic acid Chemical Properties
Melting point 200-201 °C (lit.)
alpha D20 +8° (alc)
Boiling point 437.26°C (rough estimate)
density 0.9985 (rough estimate)
refractive index 1.4460 (estimate)
storage temp. Refrigerator
solubility Solubility in methanol, very faint turbidity. Slightly soluble in alcohol, acetone, ether and very slightly soluble in chloroform.
form Solid
pka4.76±0.10(Predicted)
color White to Off-White
Water Solubility 5.889mg/L(25 ºC)
Merck 14,4857
InChIKeyDGABKXLVXPYZII-SIBKNCMHSA-N
CAS DataBase Reference83-49-8(CAS DataBase Reference)
Safety Information
Hazard Codes Xn
Risk Statements 36/37/38-40
Safety Statements 26-36/37/39-36-22-37
WGK Germany 3
RTECS FZ2050000
HS Code 29181990
MSDS Information
ProviderLanguage
Hyodeoxycholic acid English
SigmaAldrich English
ALFA English
Hyodeoxycholic acid Usage And Synthesis
Chemical PropertiesWhite Solid
UsesProtected β-Hyodeoxycholic Acid (H998105), a potential bile acid metabolite.
UsesLabelled Hyodeoxycholic Acid. Unlabelled version is isolated from pig bile. Antitumor agent
UsesIt is isolated from pig bile. Antitumor agent
UsesLabelled β-Hyodeoxycholic Acid
DefinitionChEBI: A member of the class of 5beta-cholanic acids that is (5beta)-cholan-24-oic acid substituted by alpha-hydroxy groups at positions 3 and 6.
General DescriptionHyodeoxycholic acid is a naturally occurring secondary bile acid. It is produced by the gut flora in the small intestine. Hyodeoxycholic acid is obtained from chenodeoxycholic acid during enterohepatic circulation of bile in rats.
Purification MethodsCrystallise -hyodeoxycholic acid from EtOAc or Me2CO. The K salt separates in needles from an alcoholic solution of the acid when an equivalent of KOMe is added (see lithocholic acid). [Weiland & Gumlish Hoppe Seyler's Z Physiol Chem 215 18 1933, Windaus & Bohne Justus Liebigs Ann Chem 433 278 1923, Beilstein 10 III 1631.]
Hyodeoxycholic acid Preparation Products And Raw materials
Raw materialsEthyl acetate-->Sodium sulfate-->Congo red paper-->Basic Orange 2-->Bilirubin-->Congo Red-->Sodium cholate
HYODEOXYCHOLIC ACID METHYL ESTER,HYODEOXYCHOLIC ACID METHYL ESTER 98+% Hyaluronic acid 4-(3,7-dihydroxy-10,13-dimethyl-2,3,4,5,6,7,8,9,11,12,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanoic acid Ethyl 2-(Chlorosulfonyl)acetate HYOCHOLIC ACID hyodeoxycholic acid sodium,3α,6α-Dihydroxy-5β-cholan-24-oic acid, Hyodeoxycholic acid sodium salt,HYODEOXYCHOLIC ACID SODIUM SALT Chenodeoxycholic acid Sodium deoxycholate Hyodeoxycholic acid Stearic acid Folic acid 5-BETA-CHOLANIC ACID-3-ALPHA, 6-ALPHA-DIOL DIACETATE METHYL ESTER 5-BETA-CHOLANIC ACID-3-ALPHA, 6-ALPHA, 7-ALPHA-TRIOL METHYL ESTER TAUROHYODEOXYCHOLIC ACID SODIUM SALT 5-BETA-CHOLANIC ACID-3-ALPHA, 6-ALPHA-DIOL DIACETATE 5-BETA-CHOLANIC ACID-3-ALPHA, 6-ALPHA, 7-BETA-TRIOL 5-BETA-CHOLANIC ACID-3-ALPHA, 6-ALPHA-DIOL-7-ONE Citric acid
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