N,N-Dimethylbenzamide

N,N-Dimethylbenzamide Basic information

Product Name:	N,N-Dimethylbenzamide
Synonyms:	N,N-DiMethylbenzaMide;LABOTEST-BB LT00793055;N,N-DIMETHYLBENZAMIDE;N,N-Dimethylbenzamide;Dimethylbenzmide;n,n-dimethyl-benzamid;N,N-Dimethylbenzamide98%;Benzamide, N,N-dimethyl- (6CI,8CI,9CI)
CAS:	611-74-5
MF:	C9H11NO
MW:	149.19
EINECS:	210-279-2
Product Categories:	AMIDE;Amides;Carbonyl Compounds;Organic Building Blocks
Mol File:	611-74-5.mol

N,N-Dimethylbenzamide Chemical Properties

Melting point	43-45 °C (lit.)
Boiling point	132-133 °C/15 mmHg (lit.)
density	1.0753 (rough estimate)
refractive index	1.5279 (estimate)
Fp	>230 °F
storage temp.	2-8°C(protect from light)
form	powder to lump to clear liquid
pka	-1.14±0.70(Predicted)
color	White or Colorless to Light yellow
Water Solubility	Soluble in water.
BRN	774955
InChIKey	IMNDHOCGZLYMRO-UHFFFAOYSA-N
CAS DataBase Reference	611-74-5(CAS DataBase Reference)
NIST Chemistry Reference	Benzamide, N,N-dimethyl-(611-74-5)
EPA Substance Registry System	Benzamide, N,N-dimethyl- (611-74-5)

Safety Information

Hazard Codes	Xn,Xi
Risk Statements	22-36/37/38
Safety Statements	26-36-37/39
WGK Germany	3
RTECS	CV4500000
TSCA	Yes
HS Code	29242990

MSDS Information

Provider	Language
N,N-Dimethylbenzamide	English
SigmaAldrich	English
ACROS	English
ALFA	English

N,N-Dimethylbenzamide Usage And Synthesis

Chemical Properties	white to slightly yellow cryst. low melting solid
Uses	Reagent for deoxygenation of secondary alcohols.
Synthesis Reference(s)	The Journal of Organic Chemistry, 36, p. 2721, 1971 DOI: 10.1021/jo00817a036 Journal of the American Chemical Society, 77, p. 1114, 1955 DOI: 10.1021/ja01610a010 Synthetic Communications, 12, p. 989, 1982 DOI: 10.1080/00397918208061938
General Description	N,N-Dimethylbenzamide is a hydrotropic agent and its ability to solubilize drugs with low aqueous solubility has been investigated. It reacts with PhLnI complexes (Ln-Eu, Sm, Yb) to yield benzophenone in good yields. Deuterium exchange labelling experimets on N,N-dimethylbenzamide using [IrH₂(Me₂CO)₂(PPh₃)₂]BF₄as catalyst and deuterium gas as the source of isotope has been conducted.

N,N-Dimethylbenzamide Preparation Products And Raw materials

Raw materials	N,N-Dimethylformamide-->Benzoyl chloride-->N,N-Dimethylbenzenecarbothioamide-->Benzenecarboximidic acid, N-methyl- (9CI)-->2'-Phenoxyacetophenone-->Benzaldehyde-->Dimethylamine-->Phenol-->Benzoic acid
Preparation Products	(DHQ)2PYR-->HYDROQUININE (ANTHRAQUINONE-1 4-DIYL)-->(DHQD)2PYR-->N,N-diMethyl-2-oxo-2-phenylacetaMide-->2-PHENYL-2-PENTANOL-->Guaiacol

N-(2-carbamothioylethyl)-3-hydroxy-N,4-dimethylbenzamide N-(2-carbamothioylethyl)-N,2-dimethylbenzamide N-(2-cyanoethyl)-N,3-dimethylbenzamide 4-t-Butylbenzamide N-(2-aminophenyl)-3,4-dimethylbenzamide N-(2-bromo-4-fluorophenyl)-3,4-dimethylbenzamide N-(2-bromophenyl)-2,3-dimethylbenzamide N-(4-AMINO-2-METHYLPHENYL)-4-CHLOROPHTHALIMIDE N N'-BIS(2 5-DI-T-BU-PHENYL)-3 4 9 10- N-PHTHALOYL-DL-GLUTAMIC ANHYDRIDE 4-AMINO-N,N-DIMETHYLBENZAMIDE LUCIFER YELLOW VS DILITHIUM SALT N-(2-aminophenyl)-2,5-dimethylbenzamide N-(2-cyanoethyl)-3-hydroxy-N,4-dimethylbenzamide DIETHYL 2-PHTHALIMIDOMALONATE-2-13C N-(2-amino-5-chlorophenyl)-2,4-dimethylbenzamide N-(2-carbamothioylethyl)-N,3-dimethylbenzamide N-(2-cyanoethyl)-2-hydroxy-N,5-dimethylbenzamide

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