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| | 1-Iodonaphthalene Basic information |
| | 1-Iodonaphthalene Chemical Properties |
| Melting point | 4°C | | Boiling point | 163-165 °C/15 mmHg (lit.) | | density | 1.74 g/mL at 25 °C (lit.) | | refractive index | n20/D 1.701(lit.) | | Fp | >230 °F | | storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | solubility | 0.007g/l | | form | liquid (clear) | | color | clear very deep brown-yellow | | Specific Gravity | 1.74 | | Water Solubility | Slightly soluble in water. | | Sensitive | Light Sensitive | | BRN | 1906415 | | InChIKey | NHPPIJMARIVBGU-UHFFFAOYSA-N | | CAS DataBase Reference | 90-14-2(CAS DataBase Reference) | | NIST Chemistry Reference | 1-Iodonaphthalene(90-14-2) | | EPA Substance Registry System | Naphthalene, 1-iodo- (90-14-2) |
| | 1-Iodonaphthalene Usage And Synthesis |
| Chemical Properties | clear yellow to brown liquid | | Uses | 1-Iodonaphthalene undergoes Pd catalyzed cross-coupling reaction (Stille reaction) with 2,4-dimethoxy-6-(trimethylstannyl)pyrimidine to afford 2,4-dimethoxy-6-(naphthalen-1-yl)pyrimidine. | | General Description | Ultrafast relaxation of 1-iodonaphthalene has been studied by time-resolved femtosecond pump-probe mass spectrometry. 1-Iodonaphthalene undergoes Pd catalyzed cross-coupling reaction (Stille reaction) with 2,4-dimethoxy-6-(trimethylstannyl)pyrimidine to afford 2,4-dimethoxy-6-(naphthalen-1-yl)pyrimidine. |
| | 1-Iodonaphthalene Preparation Products And Raw materials |
| Raw materials | Hydrochloric acid-->Diethyl ether-->Acetic acid-->Hexane-->Potassium iodide-->Sodium thiosulfate-->Naphthalene-->Potassium bromate-->1-Iodo-8-methylnaphthalene-->1,8-DIIODONAPHTHALENE-->1,8-DIMETHYLNAPHTHALENE | | Preparation Products | 1-Naphthalenemethanol-->7H-Benz[de]anthracen-7-one, 11-nitro--->1-(4-Bromophenyl)-naphthlene-->4,4'-Dinitrodiphenic acid-->2-(1-NAPHTHYLENE)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE-->1,1'-BINAPHTHYL |
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