|
| | 6-Methoxyisoquinoline Basic information |
| | 6-Methoxyisoquinoline Chemical Properties |
| Boiling point | 88-95?C/0.8 Torr | | density | 1.130±0.06 g/cm3(Predicted) | | storage temp. | Sealed in dry,Room Temperature | | solubility | Chloroform, Dichloromethane | | form | Oil | | pka | 6.11±0.10(Predicted) | | color | Pale Yellow | | CAS DataBase Reference | 52986-70-6(CAS DataBase Reference) |
| Hazard Codes | Xi | | Hazard Note | Irritant | | HS Code | 2933499090 |
| | 6-Methoxyisoquinoline Usage And Synthesis |
| Chemical Properties | Clear Oil | | Uses | 6-Methoxy Isoquinoline (cas# 52986-70-6) is a compound useful in organic synthesis. | | Preparation | 6-Methoxyisoquinoline synthesis: Using benzaldehyde as the starting material, m-methoxybenzaldehyde is obtained through nitration, reduction, diazotization, hydrolysis and methylation, and 3-methoxybenzaldehyde is obtained through condensation with nitromethane Shiff base and reduction of aluminum hydride -p-Phenylethylamine. The Pictet-Spengler reaction of 3-methoxyl-p-phenylethylamine and 40% aqueous formaldehyde produces 6-methoxyl-1,2,3,4-tetrahydroisoquinoline, and then obtains the target compound in dehydrogenation 6-Methoxyisoquinoline. | | Synthesis Reference(s) | Journal of the American Chemical Society, 69, p. 1939, 1947 DOI: 10.1021/ja01200a028 |
| | 6-Methoxyisoquinoline Preparation Products And Raw materials |
|
