|
| | N,N-Diethylformamide Basic information |
| | N,N-Diethylformamide Chemical Properties |
| Melting point | 176-177°C | | Boiling point | 176-177 °C (lit.) | | density | 0.908 g/mL at 25 °C (lit.) | | refractive index | n20/D 1.434(lit.) | | Fp | 141 °F | | storage temp. | Store below +30°C. | | solubility | Miscible with acetone, benzene, alcohol and ether. | | pka | -0.44±0.70(Predicted) | | form | Liquid | | color | Clear colorless to pale yellow | | BRN | 1209392 | | InChIKey | SUAKHGWARZSWIH-UHFFFAOYSA-N | | CAS DataBase Reference | 617-84-5(CAS DataBase Reference) | | EPA Substance Registry System | Formamide, N,N-diethyl- (617-84-5) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-36/37/39-37/39 | | RIDADR | UN 1993 3/PG 3 | | WGK Germany | 1 | | RTECS | LQ1925000 | | TSCA | Yes | | HazardClass | 3 | | PackingGroup | III | | HS Code | 29241990 |
| | N,N-Diethylformamide Usage And Synthesis |
| Chemical Properties | clear colorless to pale yellow liquid | | Uses | N,N-Diethylformamide is used in the synthesis of metal-organic frameworks and Diethyltrifluoromethylamine. It is also used as solvent in the preparation of porous cubic-shaped zinc oxide particles. It is involved in the preparation of quinazoline-2,4(1H,3H)-dione by reacting with o-aminonitrile. | | Uses | N,N-Diethylformamide was used in the synthesis of metal-organic frameworks. It was also used as solvent in the synthesis of porous cubic-shaped ZnO particles. | | Definition | ChEBI: N,N-diethyl-Formamide is a carboxamide. | | General Description | N,N-Diethylformamide undergoes condensation with aromatic o-aminonitriles in the presence of ZnCl2 in sealed reactor to yield quinazoline-2,4(1H,3H)-dione. |
| | N,N-Diethylformamide Preparation Products And Raw materials |
| Raw materials | Ethanediamide, N1,N1,N2,N2-tetraethyl--->N,N-diethyl-2,2-dimethylpropanamide-->Butanal, 2,2-dichloro-3-oxo--->1,1-Dichloroacetone-->1,1,3,3-Tetraethylurea-->Diethylamine | | Preparation Products | 6-CYANONICOTINIC ACID-->N,N-DIETHYL-4-NITROANILINE-->5-Nitrobenzimidazole-->N,N-DIETHYL-2-PHENYLACETAMIDE-->2,4(1H,3H)-Quinazolinedione, 6-methyl--->5-Methylbenzimidazole-->2-Methylbenzimidazole-->EthanaMine, N-[(5-broMo-3-Methoxy-2H-pyrrol-2-ylidene)Methyl]-N-ethyl- |
|