|
| | Diphenyldichloromethane Basic information |
| | Diphenyldichloromethane Chemical Properties |
| Melting point | 190 °C (decomp) | | Boiling point | 305 °C(lit.) | | density | 1.235 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.605(lit.) | | Fp | >230 °F | | storage temp. | Store below +30°C. | | solubility | Benzene (Sparingly), Chloroform (Slightly) | | form | Liquid | | color | Clear light yellow | | Water Solubility | Soluble in water (reacts), ether, benzene, ethanol, and toluene. | | BRN | 1910601 | | CAS DataBase Reference | 2051-90-3(CAS DataBase Reference) | | EPA Substance Registry System | Benzene, 1,1'-(dichloromethylene)bis- (2051-90-3) |
| Hazard Codes | C | | Risk Statements | 14-34-37 | | Safety Statements | 26-36/37/39-45 | | RIDADR | UN 3265 8/PG 2 | | WGK Germany | 3 | | F | 9-21 | | TSCA | Yes | | HazardClass | 8 | | PackingGroup | II | | HS Code | 29036990 |
| | Diphenyldichloromethane Usage And Synthesis |
| Chemical Properties | Diphenyldichloromethane is a clear light yellow liquid that is used as a precursor to other organic compounds.It is used in the synthesis of tetraphenylethylene, diphenylmethane imine hydrochloride and benzoic anhydride. | | Uses | α,α-Dichlorodiphenylmethane is a degradation product of of polychloroaromatic insecticides such as Dicofol (D436700) and DDT. It is also used as a catalyst for photodegradation of plastics. It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals. | | Preparation | Dichlorodiphenylmethane is synthesized by the condensation of benzene with carbon tetrachloride (Friedel-Crafts reaction). Add aluminum trichloride and 2/3 amount of anhydrous carbon tetrachloride into the reaction tank, cool to 10-15°C, add 1/12 amount of benzene for reaction, continue to cool to 5-10°C, add the remaining mixture of carbon tetrachloride and benzene dropwise, add after, react at 10°C for 3h. | | Synthesis Reference(s) | The Journal of Organic Chemistry, 12, p. 807, 1947 DOI: 10.1021/jo01170a012 |
| | Diphenyldichloromethane Preparation Products And Raw materials |
|
