3,5-Dinitrobenzoyl chloride

3,5-Dinitrobenzoyl chloride Basic information
Product Name:3,5-Dinitrobenzoyl chloride
Synonyms:3,5-DINITROBENZOYL CHLORIDE, FOR FLUORES CENCE;3,5-DINITROBENZOYL CHLORIDE, 98+%;Benzoyl chloride, 3,5-dinitro-;3,5-DINITROBENZOYLCHLORIDE,REAGENT;3,5-Dinitrobenzoyl Chloride [for HPLC Labeling];3,5-DINITROBENZOYL CHLORIDE, FOR HPLC LABELING 99+%;3,5-Dinitrobenzoyl chloride,99%;3,5-Dinitrobenzoyl chloride, 99% 25GR
CAS:99-33-2
MF:C7H3ClN2O5
MW:230.56
EINECS:202-750-6
Product Categories:API intermediates;Amino Group Labeling Reagents for HPLC;Hydroxyl Group Labeling Reagents for HPLC;Analytical Chemistry;HPLC Labeling Reagents;UV Detection (HPLC Labeling Reagents)
Mol File:99-33-2.mol
3,5-Dinitrobenzoyl chloride Structure
3,5-Dinitrobenzoyl chloride Chemical Properties
Melting point 68-69 °C(lit.)
Boiling point 196 °C11 mm Hg(lit.)
density 1.8836 (rough estimate)
vapor density 7.6 (vs air)
refractive index 1.6290 (estimate)
Fp 196°C/12mm
storage temp. 2-8°C
solubility Chloroform (Slightly), Ethyl Acetate (Slightly)
form Crystals or Crystalline Needles
color Yellow to beige
Water Solubility Slightly soluble in water.
Sensitive Moisture Sensitive
Merck 14,3277
BRN 990249
Stability:Stable. Incompatible with strong oxidizing agents, water, moisture, nitrates, combustible material. Refrigerate.
CAS DataBase Reference99-33-2(CAS DataBase Reference)
NIST Chemistry ReferenceBenzoyl chloride, 3,5-dinitro-(99-33-2)
EPA Substance Registry SystemBenzoyl chloride, 3,5-dinitro- (99-33-2)
Safety Information
Hazard Codes C
Risk Statements 34
Safety Statements 26-36/37/39-45-25
RIDADR UN 3261 8/PG 2
WGK Germany 3
RTECS DM6637000
21
Hazard Note Corrosive
TSCA Yes
HazardClass 8
PackingGroup II
HS Code 29163900
HS Code 29400090
MSDS Information
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3,5-Dinitrobenzoyl chloride Usage And Synthesis
Chemical Propertiesyellow-brown solid
UsesUsed in photography. This aromatic compound is used by chemists to identify alcohol components in esters and in the fluorometric analysis of creatinine.
Uses3,5-dinitrobenzoyl chloride is an important intermediate for organic synthesis.
Purification MethodsCrystallise it from CCl4 or pet ether (b 40-60o). It reacts readily with H2O and should be kept in sealed ampoules. [Beilstein 9 IV 1350.]
3,5-Dinitrobenzoyl chloride Preparation Products And Raw materials
Raw materialsThionyl chloride-->Carbon tetrachloride-->3,5-Dinitrobenzoic acid
Preparation Products(+)-DISPARLURE-->Vitamin D2-->SAPERCONAZOLE-->3,5-DINITROBENZALDEHYDE-->(S)-(+)-N-(3,5-DINITROBENZOYL)-ALPHA-PHENYLGLYCINE
3,5-DINITROBENZYL CHLORIDE 3-AMINO-BENZALDEHYDE HCL 4-(Chloromethyl)benzoyl chloride 3,5-DINITROBENZALDEHYDE 2,3,4,5-Tetrafluorobenzoyl chloride 4-Nitrobenzoyl chloride 3-NITROANILINE HYDROCHLORIDE 2-methyl-3,5-dinitrobenzoyl chloride 3-Nitrobenzyl chloride o-Toluoyl chloride 3,5-Dinitrobenzoyl chloride 3,5-Dichlorobenzoyl chloride m-Nitrobenzoyl chloride 2,4-dinitrobenzoyl chloride Mepiquat chloride 2,4,6-Trimethylbenzoyl chloride 2-Nitrobenzoyl chloride 2-​[[(2-​ethylphenyl)​(2-​hydroxyethyl)​amino]​methyl]​-​3,​3-​difluoro-Propanenitrile

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