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| | 1,2-DIHYDRONAPHTHALENE Basic information |
| | 1,2-DIHYDRONAPHTHALENE Chemical Properties |
| Melting point | −8 °C(lit.) | | Boiling point | 89 °C16 mm Hg(lit.) | | density | 0.997 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.582(lit.) | | Fp | 153 °F | | storage temp. | Sealed in dry,Room Temperature | | form | neat | | color | Colorless to Light yellow | | Water Solubility | Not miscible or difficult to mix with water. | | BRN | 1851372 | | CAS DataBase Reference | 447-53-0(CAS DataBase Reference) | | EPA Substance Registry System | Naphthalene, 1,2-dihydro- (447-53-0) |
| Safety Statements | 24/25 | | WGK Germany | 3 | | RTECS | QJ4375000 | | HS Code | 29029000 |
| | 1,2-DIHYDRONAPHTHALENE Usage And Synthesis |
| Chemical Properties | CLEAR LIGHT YELLOW TO SLIGHTLY BROWN LIQUID | | Definition | ChEBI: A dihydronaphthalene hydrogenated at C-1 and C-2. | | Synthesis Reference(s) | Tetrahedron Letters, 28, p. 2481, 1987 DOI: 10.1016/S0040-4039(00)95446-7 | | Synthesis | Dissolve 1,2-naphthoquinone (0.18 mmol) in ethanol (3 mL). NaBH4 (73 mg, 1.93 mmol) suspended in ethanol (3 mL) was added dropwise to the reaction mixture. The mixture was stirred at room temperature under nitrogen. After 1.5 hours, the mixture was poured into ice water (50 mL). Acidify the mixture with HCl (0.5 M). The mixture was extracted with CH2Cl2. The mixture was dried over magnesium sulfate. The mixture was concentrated to give 1,2-dihydroxynaphthalene. |
| | 1,2-DIHYDRONAPHTHALENE Preparation Products And Raw materials |
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