2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Basic information
Product Name:2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine
Synonyms:2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine;2-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-4,6-diphenyl-1,3,5-triazine;2,4-Diphenyl-6-(3-boronate)-1,3,5-triazine;1,3,5-Triazine, 2,4-diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-;2-[3-(4,6-Diphenyl-1,3,5-triazin-2-yl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;3-(4,6-Diphenyl-1,3,5-triazine-2-yl)phenylboronic Acid Pinacol Ester;2-dioxaborolan-2-yl)phenyl]-1;4-Diphenyl-6-[3-(4
CAS:1269508-31-7
MF:C27H26BN3O2
MW:435.33
EINECS:
Product Categories:
Mol File:1269508-31-7.mol
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Structure
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Chemical Properties
Melting point 204 °C
Boiling point 641.3±57.0 °C(Predicted)
density 1.21±0.1 g/cm3(Predicted)
form powder to crystal
pka0.92±0.10(Predicted)
color White to Almost white
Safety Information
HS Code 2934.99.4400
MSDS Information
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Usage And Synthesis
Uses2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and chemical production processes.
Synthesis123.png
15.0 g of 2-(3-Bromophenyl)-4,6-diphenyl-l,3,5- triazine (32.4 mmol), 12.3 g of bis(pinacolato)diboron (48.6 mmol), 529 mg of Pd(dppf)Cl2.CH2Cl2 (0.647 mmol), 9.53 g of potassium acetate (97.1 mmol) and 323 ml of dioxane were put into a 1-neck round flask and reacted under reflux at 90° C. for 12 hours. After completion of the reaction, the solvent was removed under reduced pressure. The produced solid was dissolved in dichloromethane and then filtered through a Celite filter and washed with dichloromethane. The solvent was removed under reduced pressure and the resultant compound was crystallized with methanol to obtain 16.0 g of solid compound (intermediate 6) (yield: 96.8%).
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Preparation Products And Raw materials
2-(3'-BroMo-biphenyl-3-yl)-4,6-diphenyl-[1,3,5]triazine 2,4-Dichloro-6-naphthalen-2-yl-[1,3,5]triazine 2-(4-Biphenylyl)-4,6-dichloro-1,3,5-triazine

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