2-Iodoxybenzoic acid

2-Iodoxybenzoic acid Basic information

Product Name:	2-Iodoxybenzoic acid
Synonyms:	2-Iodoxybenzoic Acid Stabilized (SIBX);2-Iodoxybenzoic Acid (stabilized with Benzoic Acid + Isophthalic Acid);1-Hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide 97%, 45 wt. % IBX;SIBX, 1,3-Dihydro-1,3-dioxo-1-hydroxy-1,2-benziodoxole stabilised;Iodoxybenzoic aci;2-Iodoxybenzoic acid contains stabilizer, 45 wt. % (IBX);TRILON®;TRILON®BX
CAS:	61717-82-6
MF:	C7H5IO4
MW:	280.02
EINECS:	629-407-7
Product Categories:	Fused Ring Systems;pharmacetical;API intermediates;Iodylbenzoic acid
Mol File:	61717-82-6.mol

2-Iodoxybenzoic acid Chemical Properties

Melting point	280 °C
storage temp.	under inert gas (nitrogen or Argon) at 2–8 °C
solubility	DMSO (Very Slightly, Heated)
form	powder to crystal
color	White to Almost white
Merck	14,5048
InChIKey	CQMJEZQEVXQEJB-UHFFFAOYSA-N
CAS DataBase Reference	61717-82-6(CAS DataBase Reference)

Safety Information

Hazard Codes	C,Xi,Xn
Risk Statements	22-34-44-42/43-36/37/38-20/21/22-37-35-1
Safety Statements	26-36/37/39-45-22-35
RIDADR	UN 1759 8/PG 2
WGK Germany	3
HazardClass	8
PackingGroup	Ⅱ
HS Code	29163990

MSDS Information

Provider	Language
SigmaAldrich	English

2-Iodoxybenzoic acid Usage And Synthesis

Chemical Properties	White to off-white powder, prills or agglomerates
Uses	Stabilized 2-Iodoxybenzoic Acid (SIBX)
Uses	2-Iodoxybenzoic Acid is used in the oxidation of alcohols in organic synthesis. It is also frequently used in the preparation of Dess-Martin periodinane.
Definition	ChEBI: A benziodoxole compound having hydroxy and oxo substituents at the 1-position and an oxo substituent at the 3-position.
Synthesis Reference(s)	The Journal of Organic Chemistry, 48, p. 4155, 1983 DOI: 10.1021/jo00170a070

2-Iodoxybenzoic acid Preparation Products And Raw materials

Raw materials	Sulfuric acid-->Benzoic acid-->Potassium bromate-->Isophthalic acid-->2-Iodobenzoic acid-->o-Iodobenzoic acid sodium salt-->1-Hydroxy-2-oxa-1-ioda(III)indan-3-one-->2-Iodosobenzoic acid
Preparation Products	(5-BROMOTHIOPHEN-3-YL)METHANESULFONYL CHLORIDE-->Dess-Martin periodinane-->2,4-Dimethyl-3-pentanol-->Pinacol-->2-Methyl-2-butanol

2-Iodobenzoic acid 2-IODOXYBENZOIC ACID STABILIZED MIXTURE (DESS MART Ethyl 2-(Chlorosulfonyl)acetate O-IODOXYBENZOIC ACID, 97% STABILIZED 2-IODOXYBENZOIC ACID (SIBIX) MIXTURE 2-Iodoxybenzoic acid Ascoric Acid Iodoxybenzene 2-Iodotoluene 1-HYDROXY-1,3-DIOXO-1,3-DIHYDRO-1L5-BENZO[D][1,2]IODOXOLE-4-CARBOXYLIC ACID Sodium lauroylglutamate 2-Iodosobenzoic acid Iodosobenzene Sodium lauroylsarcosinate 2-Iodobenzyl alcohol 2-IODOBENZALDEHYDE BENZOIC ACID, 2-IODYL, 1-METHYLETHYL ESTER Citric acid

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