ChemicalBook Product Catalog Chemical Reagents Organic reagents Aromatic ketones 3'-METHOXYPHENACYL BROMIDE

3'-METHOXYPHENACYL BROMIDE

3'-METHOXYPHENACYL BROMIDE Basic information
Product Name:3'-METHOXYPHENACYL BROMIDE
Synonyms:3'-Methoxyphenacyl Bromide [for HPLC Labeling];Ethanone, 2-bromo-1-(3-methoxyphenyl)-;bromomethyl 3-methoxyphenyl ketone;AKOS BBS-00003869;ALPHA-BROMO-M-METHOXYACETOPHENONE;ALPHA-BROMO-3'-METHOXYACETOPHENONE;M-METHOXYPHENACYL BROMIDE;2-BROMO-3''-METHOXYACETOPHENONE 97%
CAS:5000-65-7
MF:C9H9BrO2
MW:229.07
EINECS:225-666-1
Product Categories:Aromatics;Intermediates;Aromatic Halides (substituted);Analytical Chemistry;Carboxyl Group Labeling Reagents for HPLC;HPLC Labeling Reagents;UV Detection (HPLC Labeling Reagents)
Mol File:5000-65-7.mol
3'-METHOXYPHENACYL BROMIDE Structure
3'-METHOXYPHENACYL BROMIDE Chemical Properties
Melting point 60-62 °C(lit.)
Boiling point 215.8°C (rough estimate)
density 1.4921 (rough estimate)
refractive index 1.5500 (estimate)
storage temp. 2-8°C
solubility soluble in Methanol
form Crystalline Powder
color White to slightly yellow-green
BRN 510128
CAS DataBase Reference5000-65-7(CAS DataBase Reference)
NIST Chemistry Reference2-Bromo-3'-methoxyacetophenone(5000-65-7)
Safety Information
Hazard Codes C
Risk Statements 34-36/37-22
Safety Statements 26-27-28-36/37/39-45-34
RIDADR UN 3261 8/PG 2
WGK Germany 3
HazardClass 8
PackingGroup III
HS Code 29147000
MSDS Information
ProviderLanguage
ACROS English
SigmaAldrich English
ALFA English
3'-METHOXYPHENACYL BROMIDE Usage And Synthesis
Chemical PropertiesWHITE TO SLIGHTLY YELLOW-GREEN CRYST. POWDER
Uses2-bromo-3′-methoxyacetophenone, an alkylating agent, has been used to stabilize clopidogrel active metabolite (AM) in human plasma. It has also been used in the derivatisation of active metabolites in blood to ensure its stability during sample processing and storage.
UsesDerivatizing reagent.
PreparationObtained by reaction of bromine with 3-methoxyacetophenone in chloroform at 0° for 3 h (88%).
3'-METHOXYPHENACYL BROMIDE Preparation Products And Raw materials
Preparation Products3-Methoxyacetophenone-->5-(4-(2-(3-METHOXYPHENYL)-2-OXOETHOXY)BENZYL)THIAZOLIDINE-2,4-DIONE-->3-Methoxybenzoylacetonitrile-->2-Bromo-3′-hydroxyacetophenone-->Propanedioic acid, 2-(acetylamino)-2-[2-(3-methoxyphenyl)-2-oxoethyl]-, 1,3-diethyl ester-->3-METHOXYPHENYLGLYOXAL HYDRATE-->4-(3-Methoxyphenyl)oxazole
AURORA KA-4114 3-BROMO-1-ETHYL-1,4-DIHYDRO[1,3]DIOXOLO[4,5-G]CINNOLIN-4-ONE ALPHA,ALPHA'-DIBROMO-2,5-DIMETHOXY-1,4-DIACETYLBENZENE RARECHEM BW GA 0297 2-BROMO-2',5'-DIMETHOXYACETOPHENONE 3'-METHOXYPHENACYL BROMIDE 2-FLUORO-4-METHOXYPHENACYL BROMIDE 2'-METHOXYPHENACYL BROMIDE,2-METHOXYPHENACYL BROMIDE,2-Methoxyphenacyl bromide 98%,O-METHOXYPHENACYL BROMIDE 3-FLUORO-4-METHOXYPHENACYL BROMIDE 2-BROMO-7-METHOXY-3,4-DIHYDRONAPHTHALEN-1(2H)-ONE AURORA KA-4115 2-BROMO-3'-ACETYLOXYLACETOPHENONE 2-BROMO-2,3-DIHYDRO-4,7-DIMETHOXY-1H-INDEN-1-ONE 2-BROMO-1-(2,3-DIHYDRO-1,4-BENZODIOXIN-6-YL)ETHAN-1-ONE 2-BROMO-1-(3,4-DIHYDRO-2H-1,5-BENZODIOXEPIN-7-YL)ETHAN-1-ONE 1-(1,3-BENZODIOXOL-5-YL)-2-BROMOETHAN-1-ONE 3-Methoxyacetophenone 2-BROMO-2,3-DIHYDRO-5,6-DIMETHOXY-1H-INDEN-1-ONE
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