ChemicalBook Product Catalog Chemical Reagents Organic reagents Imide N-(3-BROMOPROPYL)PHTHALIMIDE

N-(3-BROMOPROPYL)PHTHALIMIDE

N-(3-BROMOPROPYL)PHTHALIMIDE Basic information
Product Name:N-(3-BROMOPROPYL)PHTHALIMIDE
Synonyms:AURORA KA-570;GAMMA-BROMOPROPYLPHTHALIMIDE;LABOTEST-BB LT00455358;2-(3-BROMO-PROPYL)-ISOINDOLE-1,3-DIONE;2-(3-BROMOPROPYL)-1H-ISOINDOLE-1,3(2H)-DIONE;AKOS 226-47;TIMTEC-BB SBB003049;N-(3-BROMOPROPYL)PHTHALIMIDE
CAS:5460-29-7
MF:C11H10BrNO2
MW:268.11
EINECS:226-738-5
Product Categories:alkyl bromide;N-Substituted Maleimides, Succinimides & Phthalimides;N-Substituted Phthalimides;Bifunctional CrosslinkersOrganic Building Blocks;Carbonyl Compounds;Cyclic Imides;Linkers;Peptide Synthesis
Mol File:5460-29-7.mol
N-(3-BROMOPROPYL)PHTHALIMIDE Structure
N-(3-BROMOPROPYL)PHTHALIMIDE Chemical Properties
Melting point 72-74 °C(lit.)
Boiling point 361℃
density 1.578
refractive index 1.6320 (estimate)
Fp 172℃
storage temp. Inert atmosphere,Room Temperature
solubility <1g/l
pka-2.21±0.20(Predicted)
form Crystalline Powder or Crystals
color White to light beige
BRN 157547
InChIKeyVKJCJJYNVIYVQR-UHFFFAOYSA-N
CAS DataBase Reference5460-29-7(CAS DataBase Reference)
Safety Information
Risk Statements 36/37/38
Safety Statements 22-24/25
WGK Germany 3
HS Code 29251900
MSDS Information
ProviderLanguage
ACROS English
SigmaAldrich English
ALFA English
N-(3-BROMOPROPYL)PHTHALIMIDE Usage And Synthesis
Chemical Propertieswhite powder
UsesN-(3-Bromopropyl)phthalimide is used in synthesis of several organic compounds including that of flavonoid derivatives which act as selective ABCC1 modulators with potential use as pharmacological tools for investigation of the role of ABCC1. It is also used in the synthesis of Hederagenin which is a triterpene template for the development of new antitumor compounds.
Purification MethodsPlace it in a Soxhlet and extract it with Et2O, whereby the bis-phthalimido impurity is not extracted. Evaporate the Et2O and recrystallise the residue from EtOH, aqueous EtOH or pet ether. [Gabriel & Weiner Chem Ber 21 2669 1888, Gaudry Can J Chem 31 1060 1953, Beilstein 21/10 V 1277.]
N-(3-BROMOPROPYL)PHTHALIMIDE Preparation Products And Raw materials
Preparation ProductsN,N-DIBUTYL-1,3-PROPANEDIAMINE-->N-(3-Aminopropyl)morpholine-->N,N-dipropylpropane-1,3-diamine-->1-(3-Aminopropyl)piperidine-->2-[3-(pyridin-2-ylsulfanyl)propyl]-2,3-dihydro-1H-isoindole-1,3-dione-->2-(3-(3,5-Dimethoxyphenoxy)Propyl)Isoindoline-1,3-Dione-->{[3-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propyl]sulfanyl}methanimidamide hydrobromide-->4-[3-(1,3-DIOXO-1,3-DIHYDRO-2H-ISOINDOL-2-YL)PROPOXY]BENZALDEHYDE-->ETHYL 2-(3-N-PHTHALIMIDOPROPYL)ACETOACETATE-->Diethyl [3-(N-phthalimido)propyl]phosphonate, 97%-->2-(3-(Methylthio)propyl)isoindoline-1,3-dione
SPECS AN-584/40403414 2-(3-BROMOPROPYL)-5-NITROISOINDOLINE-1,3-DIONE N-(3-BROMOPROPYL)PHTHALIMIDE N-PROPYL BENZAMIDE N-BENZYLFORMAMIDE N-METHYL-O-TOLUAMIDE TRIETHYLAMINE HYDROBROMIDE N-Benzyl-N-propylamine N,N-Diethylformamide DIMETHYLAMINE HYDROBROMIDE N-ETHYLPHTHALIMIDE CHEMBRDG-BB 9070943 BENZYLAMINE HYDROBROMIDE N-METHYL-N-(2-METHYLBENZYL)AMINE N,N-Dimethylbenzamide 2-METHYLISOINDOLIN-1-ONE N-Methylphthalimide N-N-PROPYLPHTHALIMIDE
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