Mono-tert-butyl succinate

Mono-tert-butyl succinate Basic information

Product Name:	Mono-tert-butyl succinate
Synonyms:	MONO-TERT-BUTYL SUCCINATE;mono-tert-Butyl succinate ,97%;MONO-TERT-BUTYL SUCCINATE 97％;Succiniccidono-tert-butylster;Butanedioic acid, 1-(1,1-diMethylethyl) ester;tert-Butyl hydrogen succinate;4-Tert-Butoxy-4-OxobutanoicAci;4-Tert-butoxy-4-oxobutanoic acid
CAS:	15026-17-2
MF:	C8H14O4
MW:	174.19
EINECS:
Product Categories:	C8 to C9;Carbonyl Compounds;Esters
Mol File:	15026-17-2.mol

Mono-tert-butyl succinate Chemical Properties

Melting point	51-54 °C(lit.)
Boiling point	92°C/1.5mmHg(lit.)
density	1.097±0.06 g/cm3(Predicted)
Fp	>230 °F
storage temp.	2-8°C
solubility	Chloroform (Slightly), Methanol (Sparingly)
pka	4.46±0.17(Predicted)
form	Solid
color	Yellow-brown
Water Solubility	Slightly soluble in water.
InChIKey	PCOCFIOYWNCGBM-UHFFFAOYSA-N
CAS DataBase Reference	15026-17-2

Safety Information

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-36
WGK Germany	3
HS Code	2917198090

MSDS Information

Provider	Language
SigmaAldrich	English

Mono-tert-butyl succinate Usage And Synthesis

Uses	Mono-tert-butyl Succinate is a reagent used for the synthesis of fluorinated β2- and β3-amino acids, an inhibitor of α-chymotrypsin.
Synthesis Reference(s)	Tetrahedron Letters, 32, p. 4239, 1991 DOI: 10.1016/S0040-4039(00)92137-3
General Description	mono-tert-Butyl succinate can be prepared by refluxing a mixture of succinic anhydride and N-hydroxyl succinimide in the presence of dimethylaminopyridine and triethylamine in tert-butanol and toluene.

Mono-tert-butyl succinate Preparation Products And Raw materials

Raw materials	Butanedioic acid, 1-(1,1-dimethylethyl) 4-(phenylmethyl) ester-->TERT-BUTYL METHYL SUCCINATE 97-->Di-tert-butyl Succinate-->BOC-SER-OH-->tert-Butyl bromoacetate-->tert-Butanol-->Bromoacetic acid-->Succinic acid-->tert-Butyl acetate-->Succinic anhydride
Preparation Products	TERT-BUTYL 4-HYDROXYBUTYRATE-->Butanedioic, 1-(chloromethyl)-4-t-butyl ester-->n-methoxy-n-methyl-succinamic acid tert-butyl ester

H-ASP(OTBU)-OTBU HCL Mono-tert-butyl succinate Cyhalofop-butyl FMOC-ASP(OTBU)-OPFP tert-Butyl methyl ether Tetrabutylammonium bromide Sumatriptan Buprofezin 6alpha-Methylprednisolone sodium succinate Boc-Asp-OtBu butyl rubber Phthalates Disodium succinate BUTYL OLEATE L-Aspartic acid 4-tert-butyl ester Propylamine Succinic acid iron succinate

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