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| | 2-Methoxybenzonitrile Basic information |
| | 2-Methoxybenzonitrile Chemical Properties |
| Melting point | 24.5°C | | Boiling point | 135 °C12 mm Hg(lit.) | | density | 1.093 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.5465(lit.) | | Fp | >230 °F | | storage temp. | Sealed in dry,Room Temperature | | Water Solubility | Slightly soluble in water | | form | Liquid | | color | Clear colorless to pale yellow | | BRN | 2207134 | | CAS DataBase Reference | 6609-56-9(CAS DataBase Reference) | | NIST Chemistry Reference | o-Methoxybenzonitrile(6609-56-9) |
| Hazard Codes | Xi | | Risk Statements | 36/37/38 | | Safety Statements | 26-37/39 | | RIDADR | 3276 | | WGK Germany | 3 | | HazardClass | 6.1 | | PackingGroup | III | | HS Code | 29269090 |
| | 2-Methoxybenzonitrile Usage And Synthesis |
| Chemical Properties | Colorless liquid | | Uses | 2-Methoxybenzonitrile was used in the synthesis of 5-(4′-methyl [1,1′-biphenyl]-2-yl)-1H-tetrazole. | | Preparation | o-Anisidine with sodium nitrite to make a diazonium salt solution, add it to the lead cyanide solution, and then add benzene. Put the mixture for 10-15h and carry out steam distillation, separate the benzene layer from the distillate, dry it with calcium chloride, evaporate the benzene, and distill the residue under reduced pressure, collect 120-122.5°C (1.2kPa fraction) to get 2-Methoxybenzonitrile, yield 64.5-67.3%. | | Synthesis Reference(s) | Journal of the American Chemical Society, 77, p. 109, 1955 DOI: 10.1021/ja01606a035
Synthesis, p. 641, 1992
Tetrahedron Letters, 32, p. 1007, 1991 DOI: 10.1016/S0040-4039(00)74473-X | | General Description | Surface-enhanced Raman spectra study of 2-methoxybenzonitrile has been reported. |
| | 2-Methoxybenzonitrile Preparation Products And Raw materials |
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