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| | PHENYLTRIMETHYLSILANE Basic information |
| | PHENYLTRIMETHYLSILANE Chemical Properties |
| Melting point | 166-169 °C | | Boiling point | 168-170 °C(lit.) | | density | 0.873 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.491(lit.) | | Fp | 112 °F | | storage temp. | Inert atmosphere,Room Temperature | | form | clear liquid | | Specific Gravity | 0.873 | | color | Colorless to Almost colorless | | Water Solubility | Not miscible or difficult to mix with water. | | Hydrolytic Sensitivity | 1: no significant reaction with aqueous systems | | BRN | 1855012 | | CAS DataBase Reference | 768-32-1(CAS DataBase Reference) | | NIST Chemistry Reference | Silane, trimethylphenyl-(768-32-1) | | EPA Substance Registry System | Silane, trimethylphenyl- (768-32-1) |
| Hazard Codes | Xi | | Risk Statements | 10-41-36/37/38 | | Safety Statements | 16-26-36/39-37/39 | | RIDADR | UN 1993 3/PG 3 | | WGK Germany | 3 | | TSCA | Yes | | HazardClass | 3 | | PackingGroup | III | | HS Code | 29319090 |
| | PHENYLTRIMETHYLSILANE Usage And Synthesis |
| Chemical Properties | CLEAR COLOURLESS TO GREEN LIQUID | | Uses | It is employed as intermediate for pharmaceutical and organic synthesis. | | Purification Methods | Fractionally distil the silane at atmospheric or reduced pressure (Podbielniak column p 11) and estimate it by GC with a column packed with Silicone Fluid No 710 on Chromosorb P support. [Gilman et al. J Org Chem 18 1743 1953, Maienthal et al. J Am Chem Soc 76 6392 1954, House & Respess J Organomet Chem 4 95 1965, Roberts et al. J Am Chem Soc 71 2923 1949, Freiser et al. J Am Chem Soc 75 2821 1953, Beilstein 16 I 525, 16 II 605, 16 III 1198, 16 IV 1361.] |
| | PHENYLTRIMETHYLSILANE Preparation Products And Raw materials |
| Raw materials | 1,2-BIS(TRIMETHYLSILYL)BENZENE-->DIPHENYLTETRAMETHYLDISILANE-->HEXAPHENYLDISILANE-->(DIMETHYLPHENYLSILYL)BORONIC ACID PINAC&-->TETRAPHENYLSILANE-->Hexamethyldisilane-->1,1,1-TRIMETHYL-2,2,2-TRIPHENYLDISILANE-->(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZENE | | Preparation Products | Bromotrimethylsilane-->ANTHER-->TRIMETHYLSILYLBENZENESULFONATE-->ETHYLTRIMETHYLSILANE-->N-OCTANE |
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